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激光诱导等离子体光谱法检测合金钢组分的实验研究
Alternative TitleExperimental Study on High Alloy Steel Sample by Laser-Induced Breakdown Spectroscopy
郭前进; 于海斌; 辛勇; 李晓利; 李先宏
Department工业信息学研究室
Source Publication光谱学与光谱分析
ISSN1000-0593
2010
Volume30Issue:3Pages:783-787
Indexed BySCI ; EI ; CSCD
EI Accession number20101412827132
WOS IDWOS:000275299900047
CSCD IDCSCD:3830458
Contribution Rank1
Funding Organization中国科学院知识创新重大方向项目(KGCX2-YW-126) ; 中国科学院重大科研装备项目(O8A3260301)资助
Keyword激光诱导击穿光谱技术 时间演化 高合金钢
Abstract

激光诱导击穿光谱技术(LIBS)具有无需样品制备,原位快速分析,可进行实时控制的特点使其在钢铁冶炼控制中具有巨大的实际应用价值。本文以波长为1 064 nm的Nd∶YAG调Q固体激光器为激发光源,CCD为探测器,高合金钢GBW01605—01609系列为样品,在建立的LIBS实验装置上研究激光与合金钢之间的相互作用。系统地研究了观测距离、激光能量对高合金钢样品中激光诱导击穿谱特性的影响,并分析了LIBS信号的时间分辨特性,确定了将LIBS用于合金钢微量元素定量分析时的最佳实验条件。

Other Abstract

The laser-induced breakdown spectroscopy(LIBS) technique is a fast,non-contact method with no need for any sample preparation,and can be carried out under various atmospheric conditions.These properties make LIBS applicable to process control in metallurgy.In the present paper,a series of high alloy steel GBW01605—01609 samples were determined by laser induced plasma spectroscopy,based on a Nd∶YAG Q-switched solid laser with wavelength 1 064 nm as an excitation source and CCD as detector.Experimental study on the interaction between laser and high alloy steel samples was completed.The effects on LIBS in high alloy steel such as observation distance and laser power density were systematically studied.The time-resolved spectrum of LIBS was also investigated.The optimum experiment conditions for the application of LIBS to the trace analysis in high alloy steel were obtained firstly.

Language中文
WOS HeadingsScience & Technology ; Technology
WOS SubjectSpectroscopy
WOS Research AreaSpectroscopy
Citation statistics
Document Type期刊论文
Identifierhttp://ir.sia.cn/handle/173321/5590
Collection工业信息学研究室
Corresponding Author郭前进
Affiliation1.中国科学院沈阳自动化研究所
2.北京科技大学土木与环境工程学院
Recommended Citation
GB/T 7714
郭前进,于海斌,辛勇,等. 激光诱导等离子体光谱法检测合金钢组分的实验研究[J]. 光谱学与光谱分析,2010,30(3):783-787.
APA 郭前进,于海斌,辛勇,李晓利,&李先宏.(2010).激光诱导等离子体光谱法检测合金钢组分的实验研究.光谱学与光谱分析,30(3),783-787.
MLA 郭前进,et al."激光诱导等离子体光谱法检测合金钢组分的实验研究".光谱学与光谱分析 30.3(2010):783-787.
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